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气相色谱内标法测定1,3-丙二胺及其中间体的含量 |
Determination of 1,3-Propanediamine by Capillary Gas Chromatography Internal Standard Method |
投稿时间:2008-05-20 修订日期:2008-06-16 |
DOI: |
中文关键词: 气相色谱,內标法,1,3-丙二胺 |
英文关键词:gas chromatography,internal standard,1,3-Propanediamine |
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中文摘要: |
采用毛细管气相色谱内标法测定1,3-丙二胺的含量,结果显示该方法具有分离度好、准确度高、回收率高等特点,适合1,3-丙二胺成品的质量控制,回收原料、中间体、产物的回收率都在99.10%~105.88%. |
英文摘要: |
1,3-Propanediamine was determined by capillary gas chromatography internal standard method, the results show that the method is simple, accurate and repeatable and it is suitable for quality control of 1,3-Propanediamine production. The recovery of raw material, intermediates and products was 99.10%~105.88%. |
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