气相色谱法测定托吡酯中有机溶剂残留量
Determination of Residual Organic Solvents in TOPAMAX by GC
投稿时间:2003-11-17  修订日期:2003-12-23
DOI:
中文关键词:  有机溶剂残留  托吡酯  填充柱
英文关键词:residual organic solvent  TOPAMAX  packed chromatographic column
基金项目:
作者单位
贾林 西安近代化学研究所 陕西西安 710065 
刘菊平 西安近代化学研究所 陕西西安 710065 
金水铭 西安近代化学研究所 陕西西安 710065 
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中文摘要:
      用填充柱FID-GC外标法在线检测托吡酯中4种有机溶剂残留量,通过线性、准确度、精密度、专属性、最低检测限等试验,证明此方法分离度高、灵敏、准确、简便,能满足检测要求.
英文摘要:
      Four residual organic solvents (ethanol、acetone、THF、toluene) in TOPAMAX were determined by packed chromatographic column of FID-GC via external correlation method. The analytical validation for each of residual solvents was performed with respect to the following validation characteristics: linearity, accuracy, precision, specificity, detection limit.
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